RE: the electrolyzed water

From: Klaus Wiegand (WIEGAND@lufa-sp.vdlufa.de)
Date: Wed Jul 05 2000 - 03:57:38 EDT


hello anton

>
>Here are some references on electrolyzed water that might be of interest.

thx

 Israilides CJ. Vlyssides AG. Mourafeti VN. Karvouni G.
 OLIVE OIL WASTEWATER TREATMENT WITH THE USE OF AN ELECTROLYSIS
 SYSTEM
 Bioresource Technology. 61(2):163-170, 1997 Aug.

 Olive oil wastewater (OOW), a toxic liquid associated with the
 production of olive oil, was treated by an electrochemical
 method using Ti/Pt as anode and Stainless Steel 304 as cathode.
 In this technique, sodium chloride 4% (w/v) as an electrolyte
 was added to the wastewater and the mixture was passed through
 an electrolytic cell. Due to the strong oxidizing potential Of
            (i warned about this ^^^^^^^^^)
 the chemicals produced (chlorine oxygen, hydroxyl radicals and
 other oxidants) the organic pollutants were wet oxidized to
 carbon dioxide and water. A number of experiments were run in a
 batch, laboratory-scale, pilot-plant, and the results are
 reported here. After 1 and 10 h of electrolysis at 0.26
 A/cm(2), total COD was reduced by 41 and 93%, respectively,
 total TOC was reduced by 20 and 80.4%, VSS were reduced by 1
 and 98.7%, and total phenolic compounds were reduced by 50 and
 99.4%, while the mean anode efficiency was 1960 gh(-1) A(-1)
 sq.m(-1) and 340 g h(-1) A(-1) sq.m(-1). Also, the mean energy
 consumption was 1.273 kwh per kg of COD removed and 12.3 kwh
 per kg of COD removed for 1 and 10 h, respectively. These
 results strongly indicate that this electrolytic method of
 total oxidation of OOW is not feasible. However it could be
 used as an oxidation pretreatment stage for detoxification of
 the wastewater.

 here's a technical explanation from a chemist:

 Renger G.
 MECHANISTIC AND STRUCTURAL ASPECTS OF PHOTOSYNTHETIC WATER
 OXIDATION
 Physiologia Plantarum. 100(4):828-841, 1997 Aug.

 Conclusions on the functional and structural organisation of
 photosynthetic water oxidation are gathered from a critical
 survey of the wealth of data reported in the literature and
 author's own experimental research: (1) the water oxidising
 complex (WOC) contains a tetranuclear manganese cluster of
 'dimer of dimers' structure and functional heterogeneity of the
 metal centers, (2) the four step univalent oxidative pathway
 leading to water oxidation into molecular oxygen and four
 protons comprises only manganese, tyrosine Y-Z of polypeptide
 D1 and the substrate as redox active species, (3) the redox
 transitions S-0 --> S-1 and S-1 --> S-2 are manganese centered
 whereas S-2 --> S-3 is most likely a ligand-centered reaction,
 (4) there exist several lines of evidence for a marked
 structural change that accompanies the redox transition S-2 -->
 S-3, (5) one Ca2+ is an indispensible constituent of a
 functionally competent WOC while the role of Cl- is much less
 clear and a direct participation disputable, (6) substrate
 water is most likely bound in all redox states S-0,...,S-3 and
 exchangeable with the bulk phase. The protonation state is
 determined by the redox state S-i and the protein
 microenvironment. A mechanism is proposed for water oxidation
 in the WOC that is based on three key postulates: (1) water
 oxidation takes place in the first coordination sphere of one
 manganese dimer [MnaMnb]; (2) the essential O-O bond is
 preformed in S-3 as part of a rapid redox isomerism S-3(I) <->
 S-3(II) where in S-3(II) a nuclear geometry and electronic
 configuration is attained that corresponds to a peroxidic-type
 species; and (3) S-3(II) is an 'entatic state' for the
 formation of complexed dioxygen triggered by Y-Z(OX) induced
 electron abstraction from the WOC and electronic redistribution
 to S-0(O-2). [References: 93]

 these two show, that it may very well have a "cleaning" effect
 on water:

 Kannan N. Sivadurai SN. Berchmans LJ. Vijayavalli R.
 REMOVAL OF PHENOLIC COMPOUNDS BY ELECTROOXIDATION METHOD
 Journal of Environmental Science & Health, Part A:
 Environmental Science & Engineering & Toxic & Hazardous
 Substance Control. 30(10):2185-2203, 1995.

 The present study envisages a method to remove phenol from the
 phenolic effluents by the electrooxidation under alkaline
 conditons. Synthetic effluent containing phenol (100 ppm) is
 subjected to electrolysis under various experimental conditions
 inorder to find out the optimum conditions for the removal of
 phenol. An electrolysis cell was designed with graphite
 electrodes and electrolysis was carried out under galvanostatic
 conditions keeping the total quantity of current at 0.75 A h.
 The reduction in concentration of phenol was analysed in terms
 of COD. Continuous electrolysis was also carried out at optimum
 conditions (current density: 4 A dm(-2), phenol: 100 ppm and
 supporting electrolyte. 1M NaOH) to find out the maximum
 removal of phenol. The removal of phenol from phenolic
 effluents is found to be highly efficient to the extent of
 98.55%. The electrooxidation of phenol at anode leads to the
 formation of carbon di-oxide and water. The study reveals that,
 the phenol can be almost completely oxidised at the graphite
 anode with a maximum current efficiency of 17%. It is concluded
 that, the phenol can be removed from phenolic effluents
 effectively by electrooxidation method. [References: 7]

 Allen SJ. Khader KYH. Bino M.
 ELECTROOXIDATION OF DYESTUFFS IN WASTE WATERS
 Journal of Chemical Technology & Biotechnology. 62(2):111-117,
 1995 Feb.

 An electrochemical oxidation cell is used to reduce the
 concentrations of organic dyes and chemical oxygen demand in an
 aqueous effluent. The importance of the presence of an
 electrolyte is recorded and the effects of changing both
 electrolyte concentration and initial dye concentration are
 reported. The rate of the electrooxidation process is shown to
 be a pseudo-first-order kinetic process with the rate constant
 being affected by both the electrolyte concentration and the
 dye concentration. The use of different electrolytes is
 reported. [References: 11]

i did not doubt, that these effects exist, i only said, that
20.000$ for such a device are a rip-off.

klaus

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